دانلود کتاب Mass Spectrometry in Polymer Chemistry

Combining an up-to-date insight into mass-spectrometric polymer analysis beyond MALDI with application details of the instrumentation, this is a balanced and thorough presentation of the most important and widely used mass-spectrometric methods. Written by the world's most proficient experts in the field, the book focuses on the latest developments, covering such technologies and applications as ionization protocols, tandem and liquid chromatography mass spectrometry, gas-phase ion-separation techniques and automated data processing. Chapters on sample preparation, polymer degradation and the usage of mass-spectrometric tools on an industrial scale round off the book. As a result, both entrants to the field and experienced researchers are able to choose the appropriate methods and instrumentations -- and to assess their respective strengths and limitations -- for the characterization of polymer compounds. Content: Chapter 1 Mass Analysis (pages 5–32): Gene Hart?Smith and Stephen J. BlanksbyChapter 2 Ionization Techniques for Polymer Mass Spectrometry (pages 33–56): Anthony P. GiesChapter 3 Tandem Mass Spectrometry Analysis of Polymer Structures and Architectures (pages 57–84): Vincenzo Scionti and Chrys WesdemiotisChapter 4 Matrix?Assisted Inlet Ionization and Solvent?Free Gas?Phase Separation Using Ion Mobility Spectrometry for Imaging and Electron Transfer Dissociation Mass Spectrometry of Polymers (pages 85–118): Christopher B. Lietz, Alicia L. Richards, Darrell D. Marshall, Yue Ren and Sarah TrimpinChapter 5 Polymer MALDI Sample Preparation (pages 119–147): Scott D. Hanton and Kevin G. OwensChapter 6 Surface Analysis and Imaging Techniques (pages 149–207): Christine M. Mahoney and Dr. Steffen M. WeidnerChapter 7 Hyphenated Techniques (pages 209–235): Dr. Jana Falkenhagen and Dr. Steffen WeidnerChapter 8 Automated Data Processing and Quantification in Polymer Mass Spectrometry (pages 237–280): Dr. Till Gruendling, William E. Wallace, Prof. Dr. Christopher Barner?Kowollik, Charles M. Guttman and Anthony J. KearslyChapter 9 Comprehensive Copolymer Characterization (pages 281–318): Anna C. Crecelius and Ulrich S. SchubertChapter 10 Elucidation of Reaction Mechanisms: Conventional Radical Polymerization (pages 319–372): Michael Buback, Gregory T. Russell and Philipp VanaChapter 11 Elucidation of Reaction Mechanisms and Polymer Structure: Living/Controlled Radical Polymerization (pages 373–403): Prof. Dr. Christopher Barner?Kowollik, Guillaume Delaittre, Dr. Till Gruendling and Thomas PaulohrlChapter 12 Elucidation of Reaction Mechanisms: Other Polymerization Mechanisms (pages 405–436): Grazyna Adamus and Marek KowalczukChapter 13 Polymer Degradation (pages 437–465): Paola Rizzarelli, Sabrina Carroccio and Concetto PuglisiChapter 14 Outlook (pages 467–468): Prof. Dr. Christopher Barner?Kowollik, Dr. Jana Falkenhagen, Dr. Till Gruendling and Dr. Steffen Weidner